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- MakaleAçık Erişim2024Effect of micro-arc oxidation coatings with graphene oxide and graphite on osseointegration of titanium implants-an in vivo study
Tekin, Bahar; Dundar, Serkan; Tekin, Samet; Emine Sukuroglu, Ebru; Khurshid, Zohaib; Ezgi, Yusuf; Demirci, Fatih; Faheemuddin, Muhammad
Background: This in vivo study evaluated the effect of graphene oxide and graphite coatings, coupled with the micro-arc oxidation (MAO) surface roughening technique, known for their mechanical strength, chemical stability, and antibacterial properties. The main objective was to assess the degree of improvement in osseointegration of titanium implants resulting from these interventions. Materials and methods: In this study, 32 female rats were utilized and randomly allocated into four groups (n = 8 each): machined surface titanium implants (control), those roughened by the MAO method, those coated with graphene oxide-doped MAO, and those with a graphite-doped MAO coating. Titanium implants were surgically placed in the right tibia of the rats. Rats undergoing no additional procedures during the 4-week experimental period were sacrificed at the end. Then, the implants and surrounding bone tissues were separated and embedded in acrylic blocks for reverse torque analysis. Using a digital torque device, the rotational force was applied to all samples using a hex driver and racquet until implant separation from the bone occurred, with the corresponding values recorded on the digital display. Then, statistical analysis was performed to analyze the data. Results: No statistically significant difference between the groups was observed in the biomechanical bone–implant connection levels (N/cm) (P = 0.268). Post-hoc tests were not required because no discernible differences were identified between the groups. Conclusion: Within the scope of this study, implants treated with the MAO method, along with those coated with graphene oxide- and graphite-doped MAO method, did not exhibit significant superiority in terms of osseointegration compared to machined surface titanium implants.
- MakaleYalnız künye2021Investigation of wear behavior of graphite additive composite coatings deposited by micro arc oxidation-hydrothermal treatment on AZ91 Mg alloy
Küçükosman, Rıdvan; Emine Şüküroğlu, Ebru; Totik, Yaşar; Şüküroğlu, Süleyman
Composite coatings were deposited on AZ91 magnesium alloys by micro arc oxidation (MAO) and the MAO-hydrothermal treatment (HT). The MAO process of Mg alloys was performed in the silicate/phosphate-based electrolyte with graphite particles size of 5-10 and 75 µm and then the obtained samples were submitted to hydrothermal treatment at 150°C in the graphite-ethanol mixture. The structural and morphological properties of composite coatings were analized X-ray diffraction (XRD) and scanning electron microscopy (SEM). The wear resistance was examined with ball-on-disc tribometer. The addition of graphite to the MAO electrolyte solution increased the coating thicknesses and compactness and the surface morphologies acquired relatively a homogeneous appearance. The coating surfaces were enriched in graphite by HT and the wear test results showed that the wear resistance of the graphite-doped MAO-HT composite coatings was significantly improved.
- MakaleYalnız künye2021Investigation of characterization and tribological behavior of composite oxide coatings doped with h-BN and graphite particles on ZA-27 alloy by micro-arc oxidation
Kaplan, Erdar; Sukuroglu, Ebru Emine; Cuvalci, Olkan
This paper investigates the tribological effects of composite oxide coatings grown on ZA-27 surfaces under dry sliding condition. Coating processes were conducted using three different electrolytic solutions through micro-arc oxidation (MAO) method. The base electrolytic solution without any particles as additives was labeled as MAO-Coated, whereas electrolytic solution labeled as Coated-A contained graphite particles and Coated-B contained hexagonal boron nitride (h-BN) particles incorporated into base solution. The morphology of each coated samples were analyzed using a Scanning Electron Microscope (SEM) and X-Ray Diffraction (XRD). The friction and wear tests were conducted using a pin-on-disc tester in order to evaluate the tribological behavior. Results indicated the friction coefficients of both Coated-A and Coated-B samples were lower when compared to that of uncoated ZA-27 alloy. Further comparative studies showed Coated-A samples containing graphite particles resulted in the lowest friction coefficient.