Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez

Akşit, Zeynep; Baltaci, Cemalettin

Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez

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Özet

T his study represents a high performance liquid chromatography (HPLC) method for the detection of 5-hydroxymethylfurfural in pestil, köme, jam and pekmez samples. The linearity, selectivity, decision limit, detection capability, detection limit, quantification limit, precision, recovery, ruggedness and measurement uncertainty of the method were determined. The developed method, simple and accurate, showed good recovery values (97-108%). The accuracy of the method expressed with the relative standard deviation was below 6%. The detection limit and quantification limit were 0.03 mg/kg and 0.10 mg/kg, respectively. HMF levels in pestil, köme, jam, marmalade and pekmez samples were determined using the validated method

Anahtar Kelimeler

Kimya, Tıbbi Gıda Bilimi ve Teknolojisi

RDL Kalıcı Bağlantı (PID)

https://rdlopen.rawdatalibrary.net/r/gumushane/18809Resmi atıflarda kullanılan kalıcı adres

Atıflar

TR Dizin: 5

Her kaynağın kendi saydığı toplam atıf; aktarım ve zenginleştirme sırasında alındı.

Tam Kayıt

Alan	Değer	Dil
dc.contributor.author	Akşit, Zeynep
dc.contributor.author	Baltaci, Cemalettin
dc.date.accessioned	2026-10-22T10:45:43.564836571Z
dc.date.available	2026-10-22T10:45:43.564836571Z
dc.date.issued	2016
dc.description.abstract	T his study represents a high performance liquid chromatography (HPLC) method for the detection of 5-hydroxymethylfurfural in pestil, köme, jam and pekmez samples. The linearity, selectivity, decision limit, detection capability, detection limit, quantification limit, precision, recovery, ruggedness and measurement uncertainty of the method were determined. The developed method, simple and accurate, showed good recovery values (97-108%). The accuracy of the method expressed with the relative standard deviation was below 6%. The detection limit and quantification limit were 0.03 mg/kg and 0.10 mg/kg, respectively. HMF levels in pestil, köme, jam, marmalade and pekmez samples were determined using the validated method
dc.identifier.eissn	2148-4171
dc.identifier.endpage	97
dc.identifier.issn	2149-2123
dc.identifier.issue	2
dc.identifier.startpage	91
dc.identifier.uri	https://rdlopen.rawdatalibrary.net/r/gumushane/18809
dc.identifier.volume	3
dc.language.iso	en
dc.relation.ispartof	Hittite Journal of Science and Engineering
dc.rights	info:eu-repo/semantics/closedAccess
dc.subject	Kimya, Tıbbi
dc.subject	Gıda Bilimi ve Teknolojisi
dc.title	Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez
dc.type	Article
rdl.citation.trdizin	5
rdl.source.index	TRDIZIN