Sodium silicate effect on setting properties, strength behavior and microstructure of cemented coal fly ash backfill

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Özet

Representing an engineered mixture of coal fly ash, cement and water, cemented coal fly ash backfill (CCB) is typically employed for filling the openings created after coal excavation in the earth. A high rate of productivity for coal mines requires a high early-age strength backfill design. Therefore, the use of admixtures in CCB is key for accelerating the backfill setting time and augmenting short-and long-term strength. This study offers the effect of sodium silicate (SS) as an accelerator on early age mechanical and microstructure properties of CCB. SS-based admixture was used for a dosage of 0.5, 1 and 1.5 wt% in CCB that contains 25 wt% ordinary Portland cement OPC and 75 wt% coal fly ash. Backfill setting time was done by using the Vicat system while its strength and pore structure were measured by using the uniaxial compressive strength test, and scanning electron microscopy and Hg intrusion porosimetry. Results display that use of SS in CCB increases its short-term strength gain up to 14% and shortens the mining cycle by cutting its setting time up to 58%. The microstructure analyses also indicate that CCB formulated with SS has a finer pore structure than that without admixture. The outcomes of the present study will be advantageous to evaluate both setting time and strength behavior of CCB used in coal mines, thereby causing the effective backfill plan in terms of money saving and easy operation.

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Tam Kayıt
AlanDeğerDil
dc.contributor.authorCavusoglu, Ibrahim
dc.contributor.authorYilmaz, Erol
dc.contributor.authorYilmaz, Ali Osman
dc.date.accessioned2026-10-22T10:23:08.216129887Z
dc.date.available2026-10-22T10:23:08.216129887Z
dc.date.issued2021
dc.description.abstractRepresenting an engineered mixture of coal fly ash, cement and water, cemented coal fly ash backfill (CCB) is typically employed for filling the openings created after coal excavation in the earth. A high rate of productivity for coal mines requires a high early-age strength backfill design. Therefore, the use of admixtures in CCB is key for accelerating the backfill setting time and augmenting short-and long-term strength. This study offers the effect of sodium silicate (SS) as an accelerator on early age mechanical and microstructure properties of CCB. SS-based admixture was used for a dosage of 0.5, 1 and 1.5 wt% in CCB that contains 25 wt% ordinary Portland cement OPC and 75 wt% coal fly ash. Backfill setting time was done by using the Vicat system while its strength and pore structure were measured by using the uniaxial compressive strength test, and scanning electron microscopy and Hg intrusion porosimetry. Results display that use of SS in CCB increases its short-term strength gain up to 14% and shortens the mining cycle by cutting its setting time up to 58%. The microstructure analyses also indicate that CCB formulated with SS has a finer pore structure than that without admixture. The outcomes of the present study will be advantageous to evaluate both setting time and strength behavior of CCB used in coal mines, thereby causing the effective backfill plan in terms of money saving and easy operation.
dc.description.sponsorshipKTU-RTEU
dc.description.sponsorshipTurkish Cement Manufacturers' Association
dc.description.sponsorshipTÇMB
dc.description.sponsorshipKaradeniz Teknik Üniversitesi, KTU
dc.description.sponsorshipRecep Tayyip Erdogan Üniversitesi, RTEU
dc.identifier.doi10.1016/j.powtec.2021.02.013
dc.identifier.eissn1873-328X
dc.identifier.endpage28
dc.identifier.issn0032-5910
dc.identifier.scopus2-s2.0-85101066233
dc.identifier.startpage17
dc.identifier.urihttps://rdlopen.rawdatalibrary.net/r/gumushane/14782
dc.identifier.volume384
dc.identifier.wosWOS:000634237900003
dc.language.isoen
dc.publisherElsevier B.V.
dc.relation.ispartofPowder Technology
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectCoal mine
dc.subjectCompressive strength
dc.subjectFly ash
dc.subjectMicrostructure
dc.subjectSetting time
dc.subjectSodium silicate
dc.subject.classificationEngineering, Chemical
dc.subject.classificationEngineering
dc.subject.otherCoal
dc.subject.otherCoal ash
dc.subject.otherCoal industry
dc.subject.otherCompressive strength
dc.subject.otherFly ash
dc.subject.otherPore structure
dc.subject.otherPortland cement
dc.subject.otherScanning electron microscopy
dc.subject.otherSilicates
dc.subject.otherSodium compounds
dc.subject.othercement
dc.subject.othersilicate
dc.subject.othersodium silicate
dc.subject.otherunclassified drug
dc.subject.otherEarly age strengths
dc.subject.otherLong-term strength
dc.subject.otherMicrostructure analysis
dc.subject.otherMicrostructure properties
dc.subject.otherOrdinary Portland cement
dc.subject.otherSetting properties
dc.subject.otherStrength behavior
dc.subject.otherUniaxial compressive strength
dc.subject.otheranalytic method
dc.subject.otherArticle
dc.subject.othercemented coal fly ash backfill setting time
dc.subject.otherchemical composition
dc.subject.otherchemical structure
dc.subject.othercoal mining
dc.subject.otherconcentration (parameter)
dc.subject.othermercury intrusion porosimetry
dc.subject.otherphysical parameters
dc.subject.otherCoal mines
dc.titleSodium silicate effect on setting properties, strength behavior and microstructure of cemented coal fly ash backfill
dc.typeArticle
dspace.entity.typePublication
rdl.citation.openalex146
rdl.citation.scopus149
rdl.citation.wos141
rdl.oa.statusclosed
rdl.sdgSDG09
rdl.source.indexSCOPUS
rdl.source.indexWOS
rdl.wos.indexScience Citation Index Expanded (SCI-EXPANDED)