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- MakaleYalnız künye2021Scopus SJRQ1Investigation of wear behavior of graphite additive composite coatings deposited by micro arc oxidation-hydrothermal treatment on AZ91 Mg alloy
Küçükosman, Rıdvan; Emine Şüküroğlu, Ebru; Totik, Yaşar; Şüküroğlu, Süleyman
Composite coatings were deposited on AZ91 magnesium alloys by micro arc oxidation (MAO) and the MAO-hydrothermal treatment (HT). The MAO process of Mg alloys was performed in the silicate/phosphate-based electrolyte with graphite particles size of 5-10 and 75 µm and then the obtained samples were submitted to hydrothermal treatment at 150°C in the graphite-ethanol mixture. The structural and morphological properties of composite coatings were analized X-ray diffraction (XRD) and scanning electron microscopy (SEM). The wear resistance was examined with ball-on-disc tribometer. The addition of graphite to the MAO electrolyte solution increased the coating thicknesses and compactness and the surface morphologies acquired relatively a homogeneous appearance. The coating surfaces were enriched in graphite by HT and the wear test results showed that the wear resistance of the graphite-doped MAO-HT composite coatings was significantly improved.
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İncele - MakaleYalnız künye2021Scopus SJRQ2Effects of graphene oxide addition on wear behaviour of composite coatings fabricated by plasma electrolytic oxidation (PEO) on AZ91 magnesium alloy
Kucukosman, Rıdvan; Sukuroglu, Ebru Emine; Totik, Yasar; Sukuroglu, Suleyman
Graphene oxide (GO) integrated composite coatings were deposited on AZ91 magnesium alloys by the PEO (Plasma Electrolytic Oxidation) and the treatment which has a post-PEO hydrothermal process. For the first group samples, PEO was performed in the silicate/phosphate-based electrolyte including 5–10 µm in size the GO particles synthesized using the Tour Method. For the second group samples, after PEO treatment, the post-PEO hydrothermal process was carried out in the oven in the GO-distilled water mixture containing GO produced with the same protocol. The effects of GO on wear behavior, structural and morphological features of composite coatings were examined with a pin-on-disc tribometer, X-ray diffraction (XRD), scanning electron microscopy (SEM) and Raman spectroscopy, respectively. The results showed that the addition of GO improved significantly the adhesion to the substrate material of composite coatings, increased the coating thickness and hardness. Post-PEO hydrothermal process resulted in the formation of partial a thin solid lubricant GO film on the surface of composite coatings and thus exhibited the best wear and friction resistance.
AtıfScopus26WoS24OpenAlex24İncele